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Extra resources for Inorganic Syntheses, Volume 16

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5. 6. 7. M. B. Fairy and R. J. Irving, J. Chem. ( A ) , 1966,475. J. P. Collman, N. W. Hoffman, and J. W. Hosking, Inorganic Syntheses, 12, 8 (1970). M. H. B. Stiddard, private communication. J. P. Collman, P. Farnham, and G. Dolcetti, J . Am. Chem. , 93, 1788 (1971). J. A. Osborn, F. H. Jardine, J. F. Young, and G. Wilkinson, J. Chem. ( A ) , 1966, 1711. 7. DICARBONYL+CYCLOPENTADIENYLNITROSYLMOLYBDENUM AND BIS@IHALO-tlCYCLOPENTADIENYLNITROSYLMOLYBDENUM) DERIVATIVES Submitted by D. SEDDON,' W. G.

Chem. , 35, 1531 (1961). 12. trans-BIS-(TRIPHENYHOSPHINE)CI-ILORONITROSYLIRIDIUM(1+) TETRAFLUOROBORATE NOBF [I~X(NO)[P(CGH~)~]Z]BFI(X = C1, Br) Submitted by R. J. FITZGERALDT and H. -M. W. LINT Checked by B. L. 2 tDepartment of Chemistry, Illinois Institute of Technology, Chicago, Ill. 60616. t Department of Chemistry, Northwestern University, Evanston, Ill. 60201. * The sealed reaction mixture is then heated to 100" for 24 hr with magnetic stirring. Upon cooling, a solid [largely unreacted OS~(CO)IZ] precipitates.

911. 83; mol. , 91 1 (mass spectroscopy). Properties The osmium-nitrosyl-carbonyl cluster forms green platelike crystals which are air-stable indefinitely. 1 LJ References 1. J. R. Norton, J. P. Collman, G. Dolcetti, and W. T. Robinson, Znorg. , 11, 382 (1972). 2. F. E. Hughes, J . Chem. , 35, 1531 (1961). 12. trans-BIS-(TRIPHENYHOSPHINE)CI-ILORONITROSYLIRIDIUM(1+) TETRAFLUOROBORATE NOBF [I~X(NO)[P(CGH~)~]Z]BFI(X = C1, Br) Submitted by R. J. FITZGERALDT and H. -M. W. LINT Checked by B. L. 2 tDepartment of Chemistry, Illinois Institute of Technology, Chicago, Ill.

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